HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 1-Cyclopropyl-3-(3',4'-dichlorophenyl)-4-nitropentanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Nitroethane | HCID 6587 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 2-(3,4-Dichlorophenyl)vinyl cyclopropyl ketone | HCID 54436341 | — |
| Product | 1-Cyclopropyl-3-(3',4'-dichlorophenyl)-4-nitropentanone | HCID 86734441 | — |
Reaction Steps
The procedure of Example IX using 39 g of 1-cyclopropyl-3-(3',4'-dichlorophenyl)prop-2-en-1-one, 15.5 ml of nitroethane and 2 g of sodium in 150 ml of methanol gives 41 g of 1-cyclopropyl-3-(3',4'-dichlorophenyl)-4-nitropentanone as an oily residue which is used in the crude state for the remainder of the operations.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04005103 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-d3cc967675594c55af3a046ef3f60dcd |
| Source note | uspto-grants-1977_01 |