HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 86734442, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Nitroethane | HCID 6587 | — |
| Reactant | HCID 3301250 | HCID 3301250 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Product | HCID 86734442 | HCID 86734442 | — |
Reaction Steps
The procedure of Example IX using 21 g of 1-cyclopropyl-3-(3',4'-dimethoxyphenyl)prop-2-en-1-one, 8 ml of nitroethane and 1.2 g of sodium in 80 ml of methanol gives 16 g of 1-cyclopropyl-3-(3',4'-dimethoxyphenyl)-4-nitropentanone, which is used in the crude state for the remainder of the operations.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04005103 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-60ad8fa5c38f46458ccdc543d1fd75e0 |
| Source note | uspto-grants-1977_01 |