9-Acetoxyxanthene → HCID 21482875, compound
Reaction equation
[CH2:1]([N:4]1[CH2:9][CH2:8][CH2:7][CH:6]([NH2:10])[CH2:5]1)[CH:2]=[CH2:3].C(O[CH:15]1[C:28]2[CH:27]=[CH:26][CH:25]=[CH:24][C:23]=2[O:22][C:21]2[C:16]1=[CH:17][CH:18]=[CH:19][CH:20]=2)(=O)C>C1(C)C=CC=CC=1>[CH2:1]([N:4]1[CH2:9][CH2:8][CH2:7][CH:6]([NH:10][CH:15]2[C:16]3[CH:17]=[CH:18][CH:19]=[CH:20][C:21]=3[O:22][C:23]3[C:28]2=[CH:27][CH:26]=[CH:25][CH:24]=3)[CH2:5]1)[CH:2]=[CH2:3]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
Refluxing 1-allyl-3-aminopiperidine and 9-acetoxyxanthene in dry toluene for 24 hours and working up by the procedure of Example 1 gives N-(N-allyl-3-piperidinyl)-9-xanthenylamine.
Sources & evidence
- ORD record
- ord-193dc9eb0bfe4632aa45760b64dd3ba5
- Source dataset
- uspto-grants-1977_01
- Patent number
- US04005208
Reaction notes
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