1-Cyclohexylpyrrolidin-3-amine → HCID 21482874, compound

HRID 1415561Notes

Reaction equation

HRID 1415561 reaction equation
[CH:1]1([N:7]2[CH2:11][CH2:10][CH:9]([NH2:12])[CH2:8]2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.C(O[CH:17]1[C:30]2[CH:29]=[CH:28][CH:27]=[CH:26][C:25]=2[O:24][C:23]2[C:18]1=[CH:19][CH:20]=[CH:21][CH:22]=2)(=O)C>C1(C)C=CC=CC=1>[CH:1]1([N:7]2[CH2:11][CH2:10][CH:9]([NH:12][CH:17]3[C:18]4[CH:19]=[CH:20][CH:21]=[CH:22][C:23]=4[O:24][C:25]4[C:30]3=[CH:29][CH:28]=[CH:27][CH:26]=4)[CH2:8]2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

4

Reactant 2

HCID 36700741-Cyclohexylpyrrolidin-3-amineHCID 125434549-Acetoxyxanthene

Product 1

HCID 21482874HCID 21482874, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

Refluxing N-cyclohexyl-3-aminopyrrolidine with 9-acetoxyxanthene in dry toluene for 24 hours, then working up as in Example 1 gives N-(N-cyclohexyl-3-pyrrolidinyl)-9-xanthenylamine.

Sources & evidence

ORD record
ord-299211440eee4f59926dfd432a0518ae
Source dataset
uspto-grants-1977_01
Patent number
US04005208

Reaction notes

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