HCID 10103615, compound → HCID 21482895, compound

HRID 1415564Notes

Reaction equation

HRID 1415564 reaction equation
[NH2:1][CH:2]1[CH2:7][CH2:6][CH2:5][N:4]([C:8]([O:10][CH2:11][CH3:12])=[O:9])[CH2:3]1.C(O[CH:17]1[C:30]2[CH:29]=[CH:28][CH:27]=[CH:26][C:25]=2[O:24][C:23]2[C:18]1=[CH:19][CH:20]=[CH:21][CH:22]=2)(=O)C>C1(C)C=CC=CC=1>[CH2:11]([O:10][C:8]([N:4]1[CH2:5][CH2:6][CH2:7][CH:2]([NH:1][CH:17]2[C:18]3[CH:19]=[CH:20][CH:21]=[CH:22][C:23]=3[O:24][C:25]3[C:30]2=[CH:29][CH:28]=[CH:27][CH:26]=3)[CH2:3]1)=[O:9])[CH3:12]

Participants

4

Reactant 2

HCID 10103615HCID 10103615, compoundHCID 125434549-Acetoxyxanthene

Product 1

HCID 21482895HCID 21482895, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

A mixture of 3-amino-1-carbethoxypiperidine and 9-acetoxyxanthene in dry toluene is refluxed by the procedure of Example 1 to give N-(N-ethoxycarbonyl-3-piperidinyl)-9-xanthenylamine.

Workup

  1. temperatureis refluxed by the procedure of Example 1

Sources & evidence

ORD record
ord-647d114fe16d4f01895d7ad66f8c2b6d
Source dataset
uspto-grants-1977_01
Patent number
US04005208

Reaction notes

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