HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → 1-Methoxycarbonyl-3-(2-aminophenyl)thiourea toluene-p-sulphonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | HCID 21483068 | HCID 21483068 | — |
| Product | 1-Methoxycarbonyl-3-(2-aminophenyl)thiourea toluene-p-sulphonate | HCID 21483077 | — |
| Product | 1-Methoxycarbonyl-3-(2-aminophenyl)thiourea nitrate | HCID 86734452 | — |
Reaction Steps
By proceeding in a similar manner but substituting an equimolecular quantity of nitric acid and toluene-p-sulphonic acid for the hydrochloric acid, there were obtained 1-methoxycarbonyl-3-(2-aminophenyl)thiourea nitrate, m.p. 158°-159° C. (with decomposition), and 1-methoxycarbonyl-3-(2-aminophenyl)thiourea toluene-p-sulphonate, m.p. 175°-176° C. (with decomposition), respectively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04005217 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-28330a79366a44438033aac810be552d |
| Source note | uspto-grants-1977_01 |