Benzenamine, 4-butyl-2-nitro- → HCID 21483008, compound

HRID 1415626Notes

Reaction equation

HRID 1415626 reaction equation
C([C:5]1[CH:6]=[CH:7][C:8]([NH:14][CH:15]=[O:16])=[C:9]([N+:11]([O-:13])=[O:12])[CH:10]=1)CCC.[CH:17]([O:20][C:21]([NH:23]C1C=CC(N)=C([N+]([O-])=O)C=1)=[O:22])([CH3:19])[CH3:18].C(C1C=CC(N)=C([N+]([O-])=O)C=1)CCC>>[CH:15]([NH:14][C:8]1[CH:7]=[CH:6][C:5]([NH:23][C:21]([O:20][CH:17]([CH3:19])[CH3:18])=[O:22])=[CH:10][C:9]=1[N+:11]([O-:13])=[O:12])=[O:16]

Participants

4

Reactant 3

HCID 77229Benzenamine, 4-butyl-2-nitro-HCID 126780374-Isopropoxycarbonylamino-2-nitroanilineHCID 53810500HCID 53810500, compound

Product 1

HCID 21483008HCID 21483008, compound

Procedure

In a similar manner to that described above for the preparation of 5-n-butyl-2-formamido-1-nitrobenzene but substituting an equimolecular quantity of 4-isopropoxycarbonylamino-2-nitroaniline for the 4-n-butyl-2-nitroaniline, there was obtained 2-formamido-5-isopropoxycarbonylamino-1-nitrobenzene, m.p. 168°-170° C.

Sources & evidence

ORD record
ord-c81b6d39f8e34712a7d2fb805197a90e
Source dataset
uspto-grants-1977_01
Patent number
US04005217

Reaction notes

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