HCID 21483080, compound → HCID 21482994, compound

HRID 1415631Notes

Reaction equation

HRID 1415631 reaction equation
[CH3:1][O:2][C:3]([NH:5][C:6]([NH:8][C:9]1[CH:14]=[CH:13][C:12]([NH:15][C:16]([O:18][CH:19]([CH3:21])[CH3:20])=[O:17])=[CH:11][C:10]=1[NH2:22])=[S:7])=[O:4].[CH3:23][O:24]C(NC(NC1C=CC(CCCC)=CC=1NC=O)=S)=O>>[CH3:1][O:2][C:3]([NH:5][C:6]([NH:8][C:9]1[CH:14]=[CH:13][C:12]([NH:15][C:16]([O:18][CH:19]([CH3:20])[CH3:21])=[O:17])=[CH:11][C:10]=1[NH:22][CH:23]=[O:24])=[S:7])=[O:4]

Participants

3

Reactant 2

HCID 21483080HCID 21483080, compoundHCID 54232761HCID 54232761, compound

Product 1

HCID 21482994HCID 21482994, compound

Procedure

By proceeding in a similar manner but substituting an equimolecular quantity of 1-methoxycarbonyl-3-(2-amino-4-isopropoxycarbonylaminophenyl)thiourea for the 1-methoxycarbonyl-3-(2-amino-4-n-butylphenyl)thiourea, there was obtained 1-methoxycarbonyl-3-(2-formamido-4-isopropoxycarbonylaminophenyl)thiourea, m.p. 194°-195° C. (with decomposition).

Sources & evidence

ORD record
ord-bb7040ad339f43b7b5e81137429b35aa
Source dataset
uspto-grants-1977_01
Patent number
US04005217

Reaction notes

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