反应详情

A mixture of 2-(4-methoxybenzoyl)-3-phenylbenzo[b]thiophene (12.0 g) and pyridine hydrochloride (35 g) was refluxed for thirty minutes. The hot reaction mixture was poured onto ice and the mixture transferred to a blender, homogenized, and the resulting crystals were collected by filtration, washed with water, and dried in vacuo at 80° C. yielding 11 g of the title compound.

1. temperaturewas refluxed for thirty minutes
2. additionThe hot reaction mixture was poured onto ice
3. filtrationthe resulting crystals were collected by filtration
4. washwashed with water
5. customdried in vacuo at 80° C.