p-Anisoyl chloride → HCID 15406407, compound

HRID 1415688Notes

Reaction equation

HRID 1415688 reaction equation
[C:1]1([C:7]2[C:8]3[CH:15]=[CH:14][C:13]([O:16][CH3:17])=[CH:12][C:9]=3[S:10][CH:11]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:18][O:19][C:20]1[CH:28]=[CH:27][C:23]([C:24](Cl)=[O:25])=[CH:22][CH:21]=1>>[CH3:18][O:19][C:20]1[CH:28]=[CH:27][C:23]([C:24]([C:11]2[S:10][C:9]3[CH:12]=[C:13]([O:16][CH3:17])[CH:14]=[CH:15][C:8]=3[C:7]=2[C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)=[O:25])=[CH:22][CH:21]=1

Participants

3

Reactant 2

HCID 7477p-Anisoyl chlorideHCID 15422638HCID 15422638, compound

Product 1

HCID 15406407HCID 15406407, compoundYield 91%

Procedure

3-Phenyl-6-methoxybenzo[b]thiophene and 4-methoxybenzoyl chloride were converted to the title compound by the procedure of Example 1 in 91% yield, after crystallization from methanol.

Sources & evidence

ORD record
ord-7b834b57c53a4eaba3956bb7f3bbf40d
Source dataset
uspto-grants-1999_06
Patent number
US05908859

Reaction notes

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