m-Anisoyl chloride → HCID 54272841, compound

HRID 1415689Notes

Reaction equation

HRID 1415689 reaction equation
[C:1]1([C:7]2[C:8]3[CH:15]=[CH:14][C:13]([O:16][CH3:17])=[CH:12][C:9]=3[S:10][CH:11]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:18][O:19][C:20]1[CH:21]=[C:22]([CH:26]=[CH:27][CH:28]=1)[C:23](Cl)=[O:24]>>[CH3:18][O:19][C:20]1[CH:21]=[C:22]([CH:26]=[CH:27][CH:28]=1)[C:23]([C:11]1[S:10][C:9]2[CH:12]=[C:13]([O:16][CH3:17])[CH:14]=[CH:15][C:8]=2[C:7]=1[C:1]1[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1)=[O:24]

Participants

3

Reactant 2

HCID 74374m-Anisoyl chlorideHCID 15422638HCID 15422638, compound

Product 1

HCID 54272841HCID 54272841, compoundYield 82%

Procedure

3-Phenyl-6-methoxybenzo[b]thiophene and 3-methoxybenzoyl chloride were converted to the title compound by the procedure of Example 1 in 82% yield, after crystallization from methanol.

Sources & evidence

ORD record
ord-adbd9807bfad4fe1b1f1aabbb71db3b0
Source dataset
uspto-grants-1999_06
Patent number
US05908859

Reaction notes

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