HRID1415715

反应详情

EQUATION

反应方程式

HRID 1415715 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 4-Chloro-furo[3,4-c]quinolin-3(1H)-one (500 mg), 10% Palladium on carbon (100 mg) and sodium acetate (500 mg) in 20 mL of acetic acid was hydrogenated at atmospheric pressure for 2 h. After filtration through celite, the solvent was removed in vacuo, and the residue was taken up in methylene chloride. After filtration the solvent was removed in vacuo to afford Furo[3,4-c]quinolin-3(1H)-one as a solid.

WORKUP

后处理

  1. filtrationAfter filtration through celite
  2. customthe solvent was removed in vacuo
  3. filtrationAfter filtration the solvent
  4. customwas removed in vacuo