HuagongsheHuagongshe Chemistry Print Report · For research reference only
P-Anisidine → HCID 21862856, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | P-Anisidine | HCID 7732 | — |
| Reactant | 4-(Methylsulfonyl)benzaldehyde | HCID 220376 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21862856 | HCID 21862856 | 95% |
Reaction Steps
1.00 g (5.4 mmol) of 4-methylsulfonylbenzaldehyde and 0.67 g (5.4 mmol) of 4-methoxyaniline were dissolved in 15 ml of ethanol, and the solution was heated under reflux for 1 hour. At the end of this time, the reaction solution was cooled to room temperature, and the crystals which precipitated were collected by filtration and washed with ethanol, to give 1.48 g (yield 95%) of the title compound as slightly yellow prismatic crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05908858 |
| Source dataset | uspto-grants-1999_06 |
| ORD ID | ord-e6df71cfbccb4db7a2a1e2b15d4ede7c |
| Source note | uspto-grants-1999_06 |