HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethylsilyl cyanide → alpha-(4-Methoxyphenyl)-alpha-(4-methylthioanilino)acetonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethylsilyl cyanide | HCID 82115 | — |
| Reactant | N-(4-Methoxybenzylidene)-4-methylthioaniline | HCID 21862760 | — |
| Product | alpha-(4-Methoxyphenyl)-alpha-(4-methylthioanilino)acetonitrile | HCID 21862854 | — |
Reaction Steps
Following a procedure similar to that described in Example 1(ii), but using N-(4-methoxybenzylidene)-4-methylthioaniline [prepared as described in step (i) above] and trimethylsilyl cyanide as starting materials, the title compound was obtained as a pale brown powder (yield 92%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05908858 |
| Source dataset | uspto-grants-1999_06 |
| ORD ID | ord-fa33ea44b77a4391a936bae6e149642b |
| Source note | uspto-grants-1999_06 |