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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1415756Generated: November 1, 2026

Trimethylsilyl cyanide → HCID 22443359, compound

https://huagongshe.com/reaction/1415756

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrimethylsilyl cyanideHCID 82115—
ReactantHCID 11053924HCID 11053924—
ProductHCID 22443359HCID 22443359—

Reaction Steps

Following a procedure similar to that described in Example 1(i), but using 4-methylthiobenzaldehyde and 4-fluoroaniline as starting materials, 4-fluoro-N-(4-methylthiobenzylidene)aniline was obtained in a yield of 89%. This aniline compound and trimethylsilyl cyanide were then reacted together in a similar manner to that described in Example 1(ii), to give the title compound as a slightly yellow powder (yield 47%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05908858
Source datasetuspto-grants-1999_06
ORD IDord-380e7588418a4f00b3474ec997501f42
Source noteuspto-grants-1999_06