N-bromobutanimide → HCID 21862791, compound

HRID 1415758Notes

Reaction equation

HRID 1415758 reaction equation
[F:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH:12]=[C:11]([CH3:13])[CH:10]=[C:9]2[C:14]2[CH:19]=[CH:18][C:17]([S:20]([CH3:23])(=[O:22])=[O:21])=[CH:16][CH:15]=2)=[CH:4][CH:3]=1.[Br:24]N1C(=O)CCC1=O>>[Br:24][C:12]1[N:8]([C:5]2[CH:4]=[CH:3][C:2]([F:1])=[CH:7][CH:6]=2)[C:9]([C:14]2[CH:19]=[CH:18][C:17]([S:20]([CH3:23])(=[O:22])=[O:21])=[CH:16][CH:15]=2)=[CH:10][C:11]=1[CH3:13]

Participants

3

Reactant 2

HCID 67184N-bromobutanimideHCID 21862744HCID 21862744, compound

Product 1

HCID 21862791HCID 21862791, compound

Procedure

Following a procedure similar to that described in Example 35, but using 1-(4-fluorophenyl)-4-methyl-2-(4-methylsulfonylphenyl)pyrrole (prepared as described in Example 34) and N-bromosuccinimide as starting materials, the title compound was obtained as a white powder (yield 30%), melting at 158-159° C.

Sources & evidence

ORD record
ord-c1f202d77c974a448f7325dadd26ff8f
Source dataset
uspto-grants-1999_06
Patent number
US05908858

Reaction notes

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