Methacrolein → HCID 9798131, compound

HRID 1415775Notes

Reaction equation

HRID 1415775 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH:9]([NH:12][C:13]2[CH:18]=[CH:17][C:16]([S:19](=[O:22])(=[O:21])[NH2:20])=[CH:15][CH:14]=2)[C:10]#N)=[CH:5][CH:4]=1.O=[CH:24][C:25](=C)[CH3:26]>>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[N:12]([C:13]3[CH:18]=[CH:17][C:16]([S:19](=[O:22])(=[O:21])[NH2:20])=[CH:15][CH:14]=3)[CH:24]=[C:25]([CH3:26])[CH:10]=2)=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 6562MethacroleinHCID 21862842HCID 21862842, compound

Product 1

HCID 9798131HCID 9798131, compound

Procedure

Following a procedure similar to that described in Example 1(iii), but using α-(4-methoxyphenyl)-α-(4-sulfamoylanilino)acetonitrile [prepared as described in step (ii) above] and methacrolein as starting materials, the title compound was obtained as a pale brown powder (yield 6%), melting at 163-166° C.

Sources & evidence

ORD record
ord-2ec11fb2154d4f3c90bf83a06d42ea0e
Source dataset
uspto-grants-1999_06
Patent number
US05908858

Reaction notes

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