Propanal → N,N-Bis(2-methylpropyl)prop-1-en-1-amine

HRID 1415786Notes

Reaction equation

HRID 1415786 reaction equation
[CH:1](=O)[CH2:2][CH3:3].[CH2:5]([NH:9][CH2:10][CH:11]([CH3:13])[CH3:12])[CH:6]([CH3:8])[CH3:7]>>[CH2:5]([N:9]([CH:1]=[CH:2][CH3:3])[CH2:10][CH:11]([CH3:13])[CH3:12])[CH:6]([CH3:8])[CH3:7]

Participants

3

Reactant 2

HCID 527PropanalHCID 8085Diisobutylamine

Product 1

HCID 54063094N,N-Bis(2-methylpropyl)prop-1-en-1-amineYield 29%

Procedure

Following a procedure similar to that described in Example 64(i), but using propionaldehyde and diisobutylamine as starting materials, the title compound was obtained as a colorless oily substance (yield 29%), boiling at 63-66° C./10 mmHg

Sources & evidence

ORD record
ord-8072b5351fc5453583bb366260c3af1f
Source dataset
uspto-grants-1999_06
Patent number
US05908858

Reaction notes

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