Methacrolein → HCID 9906806, compound

HRID 1415789Notes

Reaction equation

HRID 1415789 reaction equation
[CH3:1][S:2][C:3]1[CH:8]=[CH:7][C:6]([CH:9]([NH:12][C:13]2[CH:18]=[CH:17][C:16]([S:19](=[O:22])(=[O:21])[NH2:20])=[CH:15][CH:14]=2)[C:10]#N)=[CH:5][CH:4]=1.O=[CH:24][C:25](=C)[CH3:26]>>[CH3:26][C:25]1[CH:10]=[C:9]([C:6]2[CH:7]=[CH:8][C:3]([S:2][CH3:1])=[CH:4][CH:5]=2)[N:12]([C:13]2[CH:18]=[CH:17][C:16]([S:19](=[O:22])(=[O:21])[NH2:20])=[CH:15][CH:14]=2)[CH:24]=1

Participants

3

Reactant 2

HCID 6562MethacroleinHCID 53968044HCID 53968044, compound

Product 1

HCID 9906806HCID 9906806, compound

Procedure

Following a procedure similar to that described in Example 1(iii), but using α-(4-methylthiophenyl)-α-(4-sulfamoylanilino)acetonitrile [prepared as described in step (ii) above] and methacrolein as starting materials, the title compound was obtained as pale brown scaly crystals (yield 31%), melting at 172-173° C.

Sources & evidence

ORD record
ord-c2dd39ab4bc547bd812ec1401e1d542f
Source dataset
uspto-grants-1999_06
Patent number
US05908858

Reaction notes

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