Methacrolein → HCID 21862899, compound

HRID 1415801Notes

Reaction equation

HRID 1415801 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:9]([NH:12][C:13]2[CH:18]=[CH:17][C:16]([S:19](=[O:22])(=[O:21])[NH2:20])=[CH:15][CH:14]=2)[C:10]#N)[CH:5]=[CH:6][C:7]=1[Cl:8].O=[CH:24][C:25](=C)[CH3:26]>>[Cl:1][C:2]1[CH:3]=[C:4]([C:9]2[N:12]([C:13]3[CH:18]=[CH:17][C:16]([S:19](=[O:22])(=[O:21])[NH2:20])=[CH:15][CH:14]=3)[CH:24]=[C:25]([CH3:26])[CH:10]=2)[CH:5]=[CH:6][C:7]=1[Cl:8]

Participants

3

Reactant 2

HCID 6562MethacroleinHCID 21862764HCID 21862764, compound

Product 1

HCID 21862899HCID 21862899, compound

Procedure

Following a procedure similar to that described in Example 1(iii), but using α-(3,4-dichlorophenyl)-α-(4-sulfamoylanilino)acetonitrile [prepared as described in step (ii) above] and methacrolein as starting materials, the title compound was obtained as a pale brown powder (yield 33%), melting at 136-138° C.

Sources & evidence

ORD record
ord-0216dfebe26f43a1a6a177a2f51fe0d9
Source dataset
uspto-grants-1999_06
Patent number
US05908858

Reaction notes

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