HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethylsilyl cyanide → alpha-(3-Chloro-4-methoxyphenyl)-alpha-(4-sulfamoylanilino)acetonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethylsilyl cyanide | HCID 82115 | — |
| Reactant | N-(3-Chloro-4-methoxybenzylidene)-4-sulfamoylaniline | HCID 21862806 | — |
| Product | alpha-(3-Chloro-4-methoxyphenyl)-alpha-(4-sulfamoylanilino)acetonitrile | HCID 21862805 | — |
Reaction Steps
Following a procedure similar to that described in Example 1(ii), but using N-(3-chloro-4-methoxybenzylidene)-4-sulfamoylaniline [prepared as described in step (i) above] and trimethylsilyl cyanide as starting materials, the title compound was obtained as a slightly yellow powder (yield 64%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05908858 |
| Source dataset | uspto-grants-1999_06 |
| ORD ID | ord-920c3b58889e433880d1a77b15fb8da1 |
| Source note | uspto-grants-1999_06 |