4-Sulfamoylbenzaldehyde → HCID 21862799, compound
Reaction equation
[S:1]([C:5]1[CH:12]=[CH:11][C:8]([CH:9]=O)=[CH:7][CH:6]=1)(=[O:4])(=[O:3])[NH2:2].[CH2:13]([S:15][C:16]1[CH:22]=[CH:21][C:19]([NH2:20])=[CH:18][CH:17]=1)[CH3:14]>>[CH2:13]([S:15][C:16]1[CH:22]=[CH:21][C:19]([N:20]=[CH:9][C:8]2[CH:11]=[CH:12][C:5]([S:1](=[O:4])(=[O:3])[NH2:2])=[CH:6][CH:7]=2)=[CH:18][CH:17]=1)[CH3:14]Participants
3
Procedure
Following a procedure similar to that described in Example 1(i), but using 4-sulfamoylbenzaldehyde and 4-ethylthioaniline as starting materials, the title compound was obtained as a yellow powder (yield 56%).
Sources & evidence
- ORD record
- ord-9949c3312ba2469b908e2aa8335c01ec
- Source dataset
- uspto-grants-1999_06
- Patent number
- US05908858
Reaction notes
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