Sulfanilamide → N-(3,5-Dimethylbenzylidene)-4-sulfamoylaniline

HRID 1415838Notes

Reaction equation

HRID 1415838 reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]([CH:7]=[C:8]([CH3:10])[CH:9]=1)[CH:5]=O.[S:11]([C:15]1[CH:21]=[CH:20][C:18]([NH2:19])=[CH:17][CH:16]=1)(=[O:14])(=[O:13])[NH2:12]>>[CH3:1][C:2]1[CH:3]=[C:4]([CH:7]=[C:8]([CH3:10])[CH:9]=1)[CH:5]=[N:19][C:18]1[CH:20]=[CH:21][C:15]([S:11](=[O:14])(=[O:13])[NH2:12])=[CH:16][CH:17]=1

Participants

3

Reactant 2

HCID 5333SulfanilamideHCID 34225Benzaldehyde, 3,5-dimethyl-

Product 1

HCID 21862765N-(3,5-Dimethylbenzylidene)-4-sulfamoylaniline

Procedure

Following a procedure similar to that described in Example 1(i), but using 3,5-dimethylbenzaldehyde and 4-sulfamoylaniline as starting materials, the title compound was obtained as a pale yellow powder (yield 59%).

Sources & evidence

ORD record
ord-dfe7f53500804228b9dcb37ce87bbbc0
Source dataset
uspto-grants-1999_06
Patent number
US05908858

Reaction notes

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