HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 178442152, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | (Phenylmethoxy)acetaldehyde | HCID 108989 | — |
| Reactant | HCID 178444490 | HCID 178444490 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 178442152 | HCID 178442152 | — |
Reaction Steps
A solution of 100 mmol of trans-2-(4-pentylcyclohexyl)propane-1,3-diol, 100 mmol of benzyloxyacetaldehyde and 10 mmol of p-toluenesulfonic acid in 500 ml of toluene is heated at the boil on a water separator until the water separation is complete. Conventional work-up gives trans/trans-2-benzyloxymethyl-5- (4-pentylcyclohexyl)-1,3-dioxane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05911912 |
| Source dataset | uspto-grants-1999_06 |
| ORD ID | ord-2c6064e8f7fa44d082258ff1368c84d1 |
| Source note | uspto-grants-1999_06 |