HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 178442258, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 2-Pentyl-1,3-propanediol | HCID 117509 | — |
| Reactant | HCID 178520955 | HCID 178520955 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 178442258 | HCID 178442258 | — |
Reaction Steps
A solution of 100 mmol of 2-pentylpropane-1,3-diol, 100 mmol of trans-4-hydroxymethylcyclohexanecarbaldehyde and 10 mmol of p-toluenesulfonic acid in 500 ml of toluene is heated at the boil on a water separator until the water separation is complete. Conventional work-up gives trans/trans-[4-(5-pentyl-1,3-dioxan-2-yl)cyclohexyl]methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05911912 |
| Source dataset | uspto-grants-1999_06 |
| ORD ID | ord-c7e1e6adcb4d4ecab92b1c5684ca7306 |
| Source note | uspto-grants-1999_06 |