HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(2-Cyanophenyl)piperazine → HCID 19367106, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(2-Cyanophenyl)piperazine | HCID 2735875 | — |
| Reactant | 6-Chloro-2-(chloromethyl)imidazo[1,2-a]pyridine | HCID 4868389 | — |
| Product | HCID 19367106 | HCID 19367106 | — |
Reaction Steps
Following the general procedure of Example 11 and making noncritical variations, 6-chloro-2-(chloromethyl)imidazo[1,2-α]pyridine (Example 4. Step 1; 0.3373 g) and 1-(2-cyanophenyl)piperazine (Emka-Chemie; 0.347 g) give, after crystallization from dichloromethane/ethyl acetate, 0.309 g of the title compound; mp 167-169° C.; MS m/z 351, 353; IR (mineral oil) 1326, 1448, 809, 1484, 1073 cm-1 ; 1H NMR (CDCl3) δ2.79, 3.27, 3.79, 6.99, 7.12, 7.52, 8.14.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05912246 |
| Source dataset | uspto-grants-1999_06 |
| ORD ID | ord-3c49c77a038640a98a5ff0796e4862ca |
| Source note | uspto-grants-1999_06 |