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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1416378Generated: November 3, 2026

Sodium Carbonate → HCID 21709154, compound

https://huagongshe.com/reaction/1416378

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium CarbonateHCID 10340—
ReactantBromineHCID 24408—
Reactant4-Methyl-2-phenylpyridineHCID 77026—
SolventCarbon TetrachlorideHCID 5943—
ProductHCID 21709154HCID 21709154—

Reaction Steps

To a solution of 100 mg of 2-phenyl-4-methylpyridine in 2 mL of carbon tetrachloride was added 300 mg of sodium carbonate and 100 mg of bromine. The reaction mixture was stirred and irradiated with a 500 W lamp for 1 h, filtered and the solvent removed by evaporation under reduced pressure to yield 2-phenyl-4-bromomethylpyridine which was used in the next step without further purification or characterization

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05912350
Source datasetuspto-grants-1999_06
ORD IDord-b37515e4428648e1923c39737fef359a
Source noteuspto-grants-1999_06