HCID 10638264, compound → 1-(3-Nitrobenzyl)-2,4-dioxoimidazolidine-3-acetic acid

HRID 1416390Notes

Reaction equation

HRID 1416390 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([CH:20]=[CH:21][CH:22]=1)[CH2:7][N:8]1[C:12](=O)[C:11](=[O:14])[N:10]([CH2:15][C:16]([OH:18])=[O:17])[C:9]1=C)([O-:3])=[O:2].[N+](C1C=C(C=CC=1)CN1C(=O)C(=O)N(CC(O)=O)C1=S)([O-])=[O:24]>>[N+:1]([C:4]1[CH:5]=[C:6]([CH:20]=[CH:21][CH:22]=1)[CH2:7][N:8]1[CH2:12][C:11](=[O:14])[N:10]([CH2:15][C:16]([OH:18])=[O:17])[C:9]1=[O:24])([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 10638264HCID 10638264, compoundHCID 106396263-(3-Nitrobenzyl)-4,5-dioxo-2-thioxoimidazolidine-1-acetic acid

Product 1

HCID 108036281-(3-Nitrobenzyl)-2,4-dioxoimidazolidine-3-acetic acid

Procedure

The same operations as performed above in paragraphs (1) and (2) were carried out using N-3-nitrobenzyl aminoacetate as a starting material to give 1-(3-nitrobenzyl)-2,4-dioxoimidazolidine-3-acetic acid [Compound 4]. The melting point, MS, IR, NMR, and elementary analysis for the compound were:

Sources & evidence

ORD record
ord-a2a982d9503b4f039da48c3ece823ec0
Source dataset
uspto-grants-1999_06
Patent number
US05912261

Reaction notes

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