HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrimethylsilane → Silane, trimethyl(trifluoroethenyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | Chlorotrifluoroethylene | HCID 6594 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | Silane, trimethyl(trifluoroethenyl)- | HCID 11205884 | — |
Reaction Steps
Chlorotrifluoroethylene of the formula (7) is treated with n-butyl lithium and then reacted with chlorotrimethylsilane of the-formula (8) to obtain 1,1,2-trifluoro-2-trimethylsilylethylene of the formula (9). Then, without isolation, this compound (9) is reacted further with a lithium compound of the formula (10) to obtain a difluoroethylene compound of the formula (11).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05914071 |
| Source dataset | uspto-grants-1999_06 |
| ORD ID | ord-fc43b3a1500242fb9745afbfabedfb4e |
| Source note | uspto-grants-1999_06 |