2-(1,3-Dimethylbutyl)aniline → HCID 53966740, compound

HRID 1416534Notes

Reaction equation

CC(C1C=CC=CC=1N)CC(C)C.CC(C)CC(C1C=CC=CC=1N)=C.CC(C1C=CC=CC=1N)=CC(C)C.[CH3:40][CH:41]([CH3:64])[CH2:42][C:43]([C:45]1[CH:50]=[CH:49][CH:48]=[CH:47][C:46]=1[NH:51][C:52]([C:54]1[C:55]([C:60]([F:63])([F:62])[F:61])=[N:56][N:57]([CH3:59])[CH:58]=1)=[O:53])=[CH2:44]>>[CH3:44][C:43]([C:45]1[CH:50]=[CH:49][CH:48]=[CH:47][C:46]=1[NH:51][C:52]([C:54]1[C:55]([C:60]([F:62])([F:63])[F:61])=[N:56][N:57]([CH3:59])[CH:58]=1)=[O:53])=[CH:42][CH:41]([CH3:64])[CH3:40]

Participants

Reactant 4

HCID 115284412-(1,3-Dimethylbutyl)aniline

HCID 21841534HCID 21841534, compound

HCID 21841537HCID 21841537, compound

HCID 53688512HCID 53688512, compound

Product 1

HCID 53966740HCID 53966740, compoundYield 68%

Procedure

The same procedures as described in Example 2(1) were carried out except that 2-(1,3-dimethylbutyl)aniline was replaced by a 1:1 mixture of 2-(4-methyl-1-pentene-2-yl)aniline and 2-(1,3-dimethyl-1-butenyl) aniline. A mixture of N-[2-(4-methyl-1-pentene-2-yl)phenyl]-3-trifluoromethyl-1-methylpyrazole-4-carboxamide and N-[2-(1,3-dimethyl-1-butenyl)phenyl]-3-trifluoromethyl-1-methylpyrazole-4-carboxamide was obtained as a yellow crystal. Yield was 68%. Melting point was 66-74 ° C.

Sources & evidence

ORD record: ord-47198c8906fe49ce955dc56b3e099b6c
Source dataset: uspto-grants-1999_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05914344

Reaction notes

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