化工社化工社 化学情報印刷レポート · 研究参考用
Carbamic acid, ethyl ester → Methyl (3-{[(methoxycarbonyl)amino]methyl}-3,5,5-trimethylcyclohexyl)carbamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Carbamic acid, ethyl ester | HCID 5641 | — |
| 反応物 | Isophorone diamine | HCID 17857 | — |
| 生成物 | Methyl (3-{[(methoxycarbonyl)amino]methyl}-3,5,5-trimethylcyclohexyl)carbamate | HCID 3246761 | 98.1% |
反応手順
The thus-prepared crude reaction solution was analyzed by gas chromatography and it was confirmed that a urethane compound corresponding to IPDA, that is, 3-methoxycarbonylaminomethyl-3,5,5-trimethyl-1-methoxycarbonylaminocyclohexane, was produced in a yield of 98.1% based on IPDA.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05914428 |
| 出典データセット | uspto-grants-1999_06 |
| ORD ID | ord-037a08881729482397d65f6c69e1f58a |
| 出典メモ | uspto-grants-1999_06 |