HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(3-Bromophenyl)ethan-1-ol → HCID 86754134, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(3-Bromophenyl)ethan-1-ol | HCID 2734090 | — |
| Reactant | 5-{2-[2-(3-Chloro-phenyl)-2-hydroxy-ethylamino]-propyl}-benzo[1,3]dioxole-2,2-dicarboxylic acid | HCID 4281355 | — |
| Product | HCID 86754134 | HCID 86754134 | — |
Reaction Steps
The title compound was prepared as a brown oil from 5-{2-[2-(3-chloro-phenyl)-2-hydroxy-ethylamino]-propyl}-benzo[1,3]dioxole-2,2-dicarboxylic acid and 2-(3-bromophenyl)ethanol according to the procedure of Example 1; 1H NMR (300 MHz, CDCl3): δ 1.12 (m, J=6.3 Hz, 3H), 2.79 (m, 8H), 3.5 (m 2H), 4.18 (s, 1H, OH), 5.56 (m, 1H), 6.8 (m, 3H), 7.0 (m, 4H), 7.33 (m, 4H), 7.5 (m, 4H), 8.5 (m, 1H, NH); MS (ES) m/z (relative intensity): 788 (M+ +H, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05914339 |
| Source dataset | uspto-grants-1999_06 |
| ORD ID | ord-516814bbfa554c2e816eb8c041811488 |
| Source note | uspto-grants-1999_06 |