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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1416783Generated: November 3, 2026

2-(3-Bromophenyl)ethan-1-ol → HCID 86754134, compound

https://huagongshe.com/reaction/1416783

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-(3-Bromophenyl)ethan-1-olHCID 2734090—
Reactant5-{2-[2-(3-Chloro-phenyl)-2-hydroxy-ethylamino]-propyl}-benzo[1,3]dioxole-2,2-dicarboxylic acidHCID 4281355—
ProductHCID 86754134HCID 86754134—

Reaction Steps

The title compound was prepared as a brown oil from 5-{2-[2-(3-chloro-phenyl)-2-hydroxy-ethylamino]-propyl}-benzo[1,3]dioxole-2,2-dicarboxylic acid and 2-(3-bromophenyl)ethanol according to the procedure of Example 1; 1H NMR (300 MHz, CDCl3): δ 1.12 (m, J=6.3 Hz, 3H), 2.79 (m, 8H), 3.5 (m 2H), 4.18 (s, 1H, OH), 5.56 (m, 1H), 6.8 (m, 3H), 7.0 (m, 4H), 7.33 (m, 4H), 7.5 (m, 4H), 8.5 (m, 1H, NH); MS (ES) m/z (relative intensity): 788 (M+ +H, 100).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05914339
Source datasetuspto-grants-1999_06
ORD IDord-516814bbfa554c2e816eb8c041811488
Source noteuspto-grants-1999_06