HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxyphenol → HCID 54052515, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxyphenol | HCID 9007 | — |
| Reactant | 3-Bromobiphenyl | HCID 16449 | — |
| Product | HCID 54052515 | HCID 54052515 | — |
Reaction Steps
Under the Ullmann conditions used in Example 8, steps A and B, above, 13.3 g of 3-methoxyphenol (107 mmole) was condensed with 1-bromo-3-phenylbenzene, giving, after purifying over silica gel, (0-30% EtOAc in hexane gradient) 17.8 g (60%) of 3-(3-phenylphenoxy)anisole as a crystalline solid, melting at 41-42° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05916922 |
| Source dataset | uspto-grants-1999_06 |
| ORD ID | ord-8bab97e5153a48eb86304a46b2de5bc5 |
| Source note | uspto-grants-1999_06 |