HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(7-Oxooxepan-2-yl)propanenitrile → 8-Cyano-octanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(7-Oxooxepan-2-yl)propanenitrile | HCID 11768938 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 8-Cyano-octanoic acid | HCID 11084300 | — |
Reaction Steps
In a reactor with a catalyst composed of palladium on carbon at 5% deposited on the walls, 167 g of 7-cyanoethyl-2-oxepanone are heated to 500° C. in a hydrogen atmosphere, collecting 1 g/minute of liquid condensed product mainly formed by 8-cyanooctanoic acid with 95% lactone conversion and 80% selectivity.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05917067 |
| Source dataset | uspto-grants-1999_06 |
| ORD ID | ord-06bb0a1806d24dfe947b9b01a1cf012e |
| Source note | uspto-grants-1999_06 |