4-Cyanobenzoyl chloride → HCID 15407873, compound

HRID 1417070Notes

Reaction equation

HRID 1417070 reaction equation
[C:1]([C:3]1[CH:19]=[CH:18][C:6]([C:7]([N:9]([CH3:17])[CH2:10][C:11]2[CH:16]=[CH:15][N:14]=[CH:13][CH:12]=2)=O)=[CH:5][CH:4]=1)#[N:2].[C:20]([C:22]1[CH:30]=[CH:29][C:25](C(Cl)=O)=[CH:24][CH:23]=1)#[N:21]>>[C:1]([C:3]1[CH:19]=[CH:18][C:6]([C:7]2[N:9]([CH3:17])[C:10]([C:11]3[CH:16]=[CH:15][N:14]=[CH:13][CH:12]=3)=[C:20]([C:22]3[CH:30]=[CH:29][CH:25]=[CH:24][CH:23]=3)[N:21]=2)=[CH:5][CH:4]=1)#[N:2]

Participants

3

Reactant 2

HCID 801724-Cyanobenzoyl chlorideHCID 15407881HCID 15407881, compound

Product 1

HCID 15407873HCID 15407873, compound

Procedure

4-Cyano-N-methyl-N-(4-picolyl)benzamide The title compound was prepared using the same procedure as described in Example 2, step (b) except using 4-cyanobenzoyl chloride: 1H NMR (CDCl3): d 8.49 (dd, 2H); 7.86-7.04 (m, 6H); 4.70 and 4.43 (two br s, 2H); 3.08 and 2.89 (two br s, 3H).

Sources & evidence

ORD record
ord-1ff28bfc3e584cef8a18dbece02cb89a
Source dataset
uspto-grants-1999_06
Patent number
US05916891

Reaction notes

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