Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Product | Homophthalic anhydride | HCID 12801 | — |
Reaction Steps
A solution of homophthalic anhydride (324 mg, 2 mmoles) and triethylamine (0.021 ml, 0.15 mmoles) is prepared in DMF (5 ml) and added to each packet. After heating at 80° C. for 16 hrs the packets are then washed with DMF (3×30 ml) and DCM (3×30 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05916899 |
|---|
| Source dataset | uspto-grants-1999_06 |
|---|
| ORD ID | ord-f10ee9ff02d9409b8a5ad24d7869004b |
|---|
| Source note | uspto-grants-1999_06 |
|---|
