HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 9837522, compound → HCID 21845565, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 9837522 | HCID 9837522 | — |
| Reactant | 2-Bromo-1-(3,4-dihydroxy-5-nitro-phenyl)-ethanone | HCID 21845596 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21845565 | HCID 21845565 | — |
Reaction Steps
A mixture of 0.24 g of N-(aminothioxomethyl)-4-methyl-benzenesulfonamide and 0.2 g of 2-bromo-1-(3,4-dihydroxy-5-nitrophenyl)ethanone was dissolved in 5 ml of ethanol and boiled under reflux for 1 h. 0.26 g of N-[4-(3,4-dihydroxy-5-nitro-phenyl)-thiazol-2-yl]-4-methyl-benzenesulfonamide separated as red crystals upon cooling.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05877193 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-53a0b64789e24a0a8379b511b3f947b8 |
| Source note | uspto-grants-1999_03 |