HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-[4-(4-Nitrophenoxy)butyl]-1H-isoindole-1,3(2H)-dione → HCID 3030019, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-[4-(4-Nitrophenoxy)butyl]-1H-isoindole-1,3(2H)-dione | HCID 16105142 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 3030019 | HCID 3030019 | — |
Reaction Steps
A suspension of 6.8 g of 2-[4-(4-nitro-phenoxy)butyl]-1H-isoindole-1,3(2H)-dione (Example 33) in 200 ml of ethanol is treated with 500 mg of 10% Pd on carbon, and reduced in a Parr hydrogenator. After filtration, concentration of the filtrate gives the desired product, m.p. 119°-121° C.; yield 4.3 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05877196 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-6de960758f5445b888ed99468905e9ac |
| Source note | uspto-grants-1999_03 |