HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → HCID 178506628, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | 2,2'-Bipyridine | HCID 1474 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Potassium | HCID 5462222 | — |
| Reactant | HCID 86753407 | HCID 86753407 | — |
| Reactant | HCID 178419084 | HCID 178419084 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178506628 | HCID 178506628 | — |
Reaction Steps
For potassium (2,2'-bipyridine) oxodiperoxovanadium (V), vanadium pentoxide (0.91 g) and potassium hydroxide (0.65 g) are dissolved in water (10 ml), cooled, and, if necessary, the dissolution is completed with a small amount of hydrogen peroxide. To the clear, cooled solution, hydrogen peroxide (10 ml) and 2,2'-bipyridine (1.6 g) dissolved in ethanol (7-8 ml) are added. Pure crystals are obtained as described for the analogous oxalato-derivative of potassium. Potassium (1,10-phenanthroline) vanadium (V) can be obtained similarly.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05877210 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-640e160dc4d144fd953db6846cb5ad84 |
| Source note | uspto-grants-1999_03 |