Methyl iodide → HCID 54014138, compound

HRID 1417503Notes

Reaction equation

[CH3:1][C:2]1[C:14]2[C:13]3[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=3)[NH:7][C:6]=2[C:5]([S:15][CH3:16])=[C:4]([CH2:17][C:18]([O:20][CH:21]([CH3:23])[CH3:22])=[O:19])[CH:3]=1.[CH3:24]I>>[CH3:1][C:2]1[C:14]2[C:13]3[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=3)[N:7]([CH3:24])[C:6]=2[C:5]([S:15][CH3:16])=[C:4]([CH2:17][C:18]([O:20][CH:21]([CH3:23])[CH3:22])=[O:19])[CH:3]=1

Participants

Reactant 2

HCID 6328Methyl iodide

HCID 53689308HCID 53689308, compound

Product 1

HCID 54014138HCID 54014138, compoundYield 80%

Procedure

Following a procedure and using relative proportions of starting materials similar to those described in Example 4, but using isopropyl (4-methyl-1-methylthiocarbazol-2-yl)acetate and methyl iodide as starting materials, the title compound was obtained in a yield of 80% as an oil.

Sources & evidence

ORD record: ord-e4f4e12d3eff49218be1864c8b078dda
Source dataset: uspto-grants-1999_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05877199

Reaction notes

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