Acrylic Acid → Trichlorogermylpropionic acid

HRID 1417598Notes

Reaction equation

[Cl:1][GeH:2]([Cl:4])[Cl:3].[C:5]([OH:9])(=[O:8])[CH:6]=[CH2:7]>>[Cl:1][Ge:2]([CH:6]([CH3:7])[C:5]([OH:9])=[O:8])([Cl:4])[Cl:3]

Participants

Reactant 2

HCID 6581Acrylic Acid

HCID 70900CID 70900

Product 1

HCID 13587901Trichlorogermylpropionic acid

Procedure

Trichlorogermane (Cl3GeH) was added to acrylic acid (CH2CHCOOH) to obtain trichlorogermylpropionic acid (Cl3GeCH2CH2COOH). It was hydrolyzed to synthesize an organogermanium compound (1). In the same manner were synthesized organogermanium compounds (2) to (51).

Sources & evidence

ORD record: ord-827b4ac667704e19b037162cd4fbe701
Source dataset: uspto-grants-1999_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05877311

Reaction notes

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