HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycinamide → HCID 54569709, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycinamide | HCID 69020 | — |
| Reactant | 1,3-Dichloro-2-isothiocyanatobenzene | HCID 123239 | — |
| Product | HCID 54569709 | HCID 54569709 | — |
Reaction Steps
2-[3-(2,6-Dichlorophenyl)-thioureido]-acetamide was prepared by the procedure described in Example 2 using 40.8 g of 2,6-dichlorophenyl-isothiocyanate and 29.6 g of glycinamide. The product was obtained (54 g) as a solid, m.p. 189°-191° C. Mass spectrum (+FAB, [M+H]+) m/z 278/280/282. This intermediate was used in the next paragraph without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05877324 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-d529689878f54aaf88a86a21daa3a62d |
| Source note | uspto-grants-1999_03 |