Iodoethane → HCID 44295455, compound

Participants

Reaction Steps

The title compound was prepared by the procedure described in Example 2 using 27.8 g of 2-[3-(2,6-dichlorophenyl)-thioureido]-acetamide and 31.2 g of ethyl iodide. 12.8 g of the title compound was obtained, m.p. 122°-124° C. Anal. Calcd. for. C11H10Cl2N2O S: C, 45.69; H, 3.49; N, 9.69. Found: C, 45.62; H, 3.33; N, 9.43. Mass spectrum (+FAB, [M+H]+) m/z 289/291/293. 1H-NMR (DMSO-d6 ; 400 MHz) δ7.72 (s, 1 H), 7.70 (s, 1 H), 7.58 (t, 1 H), 4.50 (s, 2 H), 3.10 (q, 2 H), and 1.27 ppm (t, 3 H).

Provenance & Evidence