HCID 67573795, compound → HCID 67584118, compound

Participants

Reaction Steps

2.46 g (4.3 mmol) of allyl 4-[4-(1-adamantyl)-3-methoxyethoxymethoxybenzoyloxy]benzoate, 40 ml of dioxane and 492 mg of palladium-on-charcoal (10%) were introduced into a reactor. The mixture was hydrogenated at 40° C. and at a pressure of 7 bar for three hours. The catalyst was filtered off and the filtrate was evaporated to dryness. The solid obtained was recrystallized from methanol, filtered off and dried. 1.57 g (76%) of the expected acid, having a melting point of 212°-4° C., was recovered.

Provenance & Evidence