HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12322843, compound → Ethyl 2-(1,2,3,4-tetrahydronaphthalen-1-yl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12322843 | HCID 12322843 | — |
| Reactant | HCID 12322844 | HCID 12322844 | — |
| Product | Ethyl 2-(1,2,3,4-tetrahydronaphthalen-1-yl)acetate | HCID 12322859 | — |
Reaction Steps
Following the general procedure of EXAMPLE 64 and making non-critical variations but starting with (E)-1-carbethoxymethylene-1,2,3,4-tetrahydronaphthalene (CVII-A, EXAMPLE 63), ethyl 1-(3,4-dihydronaphthyl)acetate (CVII-B, EXAMPLE 63) and (Z)-1-carbethoxymethylene-1,2,3,4-tetrahydronaphthalene (CVII-C, EXAMPLE 63), the title compound is obtained, NMR (CDCl3, TMS) 7.25-7.05, 4.16, 3.38-3.30, 2.83-1.64 and 1.27 δ.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05877317 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-c0d1b698792b4f88bc5e1dc13ebc25cc |
| Source note | uspto-grants-1999_03 |