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HRID1417853

反应详情

EQUATION

反应方程式

HRID 1417853 的结构方程式

REACTANTS

反应物

5
结构：NS(=O)(=O)c1ccc(F)cc1
HCID120231

4-Fluorobenzenesulfonamide

C6H6FNO2S

结构：NS(=O)(=O)c1ccc(N2CCNCC2)cc1
HCID901897

4-piperazin-1-ylbenzenesulfonamide

C10H15N3O2S

结构：C[C@@H]1CNC[C@H](C)N1
HCID6950261

rel-(2R,6S)-2,6-Dimethylpiperazine

C6H14N2

2 次

结构：CC1CN(c2ccc(S(N)(=O)=O)cc2)CC(C)N1
HCID23288831

未命名化合物

结构：CC1COC(CCCl)c2ccccc21
HCID23288938

未命名化合物

PRODUCTS

生成物

1
结构：C[C@@H]1CN(c2ccc(S(N)(=O)=O)cc2)C[C@H](C)N1CC[C@@H]1OCCc2ccccc21
HCID21308103

未命名化合物

PROCEDURE

实验过程

Following the general procedure of EXAMPLE 49 and making non-critical variations 2-(isochroman-1-yl)ethanol-O-methanesulfonate (LXXX, 0.412 g) and 4-(3,5-dimethylpiperazin-1-yl)benzenesulfonamide [(IV), 0.433 g; prepared from 4-fluorobenzenesulfonamide, III, and cis-2,6-dimethylpiperazine, II (Aldrich), by the method of EXAMPLE 47] gives the title compound; mp 170°-175°(decomp)°; MS (m/z) 429; IR (mineral oil) 1153, 1596, 1325, 1162 and 1096 cm-1.