Water → HCID 131721141, compound

HRID 1417868Notes

Reaction equation

HRID 1417868 reaction equation
[NH2:1][CH2:2][CH2:3][CH2:4][Si:5](OCC)(OCC)[O:6]CC.O.[C:16]([OH:29])(=[O:28])[CH2:17]CCCCCCCCCC>C(O)C>[NH2:1][CH2:2][CH2:3][CH2:4][SiH2:5][O:6][CH2:17][CH:16]([OH:28])[OH:29]

Participants

5

Reactant 3

HCID 962WaterHCID 3893Lauric Acid2×HCID 13521(3-Aminopropyl)triethoxysilane

Product 1

HCID 131721141HCID 131721141, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

0.10 mol of 3-aminopropyltriethoxysilane is charged under a nitrogen atmosphere to a sulfonating flask. 0.20 mol of water and 0.10 mol of lauric acid are then added with thorough stirring, and stirring is continued at room temperature for one hour. The salt derived from lauric acid and 3-aminopropyldihydroxyethoxysilane [Compound (118)] is obtained in quantitative yield as an 80% solution in ethanol.

Sources & evidence

ORD record
ord-81783c3ef90f4f3fb64bb3ec00c3f203
Source dataset
uspto-grants-1999_03
Patent number
US05879436

Reaction notes

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