HCID 15860250, compound → HCID 10814454, compound

HRID 1417938Notes

Reaction equation

HRID 1417938 reaction equation
[S:1]([O:5][C:6]1[CH:23]=[CH:22][C:21]2[C@@H:20]3[C@H:11]([C@H:12]4[C@@:16]([CH2:18][CH2:19]3)([CH3:17])[C:15](C(=O)NCCCCCCC)=[CH:14][CH2:13]4)[CH2:10][CH2:9][C:8]=2[CH:7]=1)(=[O:4])(=[O:3])[NH2:2].OC1C=CC2[C@@H]3[C@H]([C@H]4[C@@](CC3)(C)[C@@H]([NH:53][C:54](=[O:62])[CH2:55][CH2:56][CH2:57][CH2:58][CH2:59][CH2:60][CH3:61])CC4)CCC=2C=1>>[S:1]([O:5][C:6]1[CH:23]=[CH:22][C:21]2[C@@H:20]3[C@H:11]([C@H:12]4[C@@:16]([CH2:18][CH2:19]3)([CH3:17])[C@@H:15]([NH:53][C:54](=[O:62])[CH2:55][CH2:56][CH2:57][CH2:58][CH2:59][CH2:60][CH3:61])[CH2:14][CH2:13]4)[CH2:10][CH2:9][C:8]=2[CH:7]=1)(=[O:4])(=[O:3])[NH2:2]

Participants

3

Reactant 2

HCID 15860250HCID 15860250, compoundHCID 69990480HCID 69990480, compound

Product 1

HCID 10814454HCID 10814454, compoundYield 50%

Procedure

Sulfamates 11a (50%) were prepared by using the procedure outlined in Example 1 for the synthesis of sulfamate (5a), but using compound 10a instead of compound 4a.

Sources & evidence

ORD record
ord-d0be76d7e3dd461689e23f492ebc5b40
Source dataset
uspto-grants-1999_03
Patent number
US05880115

Reaction notes

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