HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethanolamine → HCID 70344994, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethanolamine | HCID 8113 | — |
| Reactant | HCID 70187132 | HCID 70187132 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70344994 | HCID 70344994 | 21% |
Reaction Steps
A mixture of 4-[4'-(ethoxycarbonylmethoxy)anilino]6-(3'-methylanilino)pyrimidine (0.30 g) and diethanolamine (0.5 g) in ethanol (10 ml) was refluxed for 8 hours. The product so obtained was chromatographed on silica to give 4-[4'-{N,N-di-(2-hydroxyethyl)carbamoylmethoxy}anilino]6-(3'-methylanilino)pyrimidine in 21% yield, m.p. 160°-162° C.;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05880130 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-52ae1214f67a43b5b29bba4dae288b65 |
| Source note | uspto-grants-1999_03 |