HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → 4-(4-Chlorophenyl)-2-fluoro-4-methylpent-2-enol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | Methyl 4-(4-chlorophenyl)-2-fluoro-4-methylpent-2-enoate | HCID 54161401 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 4-(4-Chlorophenyl)-2-fluoro-4-methylpent-2-enol | HCID 53791045 | 92% |
Reaction Steps
The method of Example 6 was repeated using methyl 4-(4-chlorophenyl)-2-fluoro-4-methylpent-2-enoate (Example 3) (0.56 g), diethyl ether (20 ml) and lithium aluminium hydride (0.21 g) to yield the title compound (0.35 g, 92%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05880162 |
| Source dataset | uspto-grants-1999_03 |
| ORD ID | ord-313e3d51296148618919c1cf031aef9a |
| Source note | uspto-grants-1999_03 |